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Kataev S.S.

Permskoe kraevoe biuro sudebno-meditsinskoĭ ékspertizy

Dvorskaia O.N.

Permskaia gosudarstvennaia farmatsevticheskaia akademiia

The application of the solid phase extraction technique to the analysis of blood for the presence of narcotic and pharmaceutical substances

Authors:

Kataev S.S., Dvorskaia O.N.

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Journal: Forensic Medical Expertise. 2012;55(4): 38‑42

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THE APPLICATION OF THE SOLID PHASE EXTRACTION TECHNIQUE TO THE ANALYSIS OF BLOOD FOR THE PRESENCE OF NARCOTIC AND PHARMACEUTICAL SUBSTANCES
THE APPLICATION OF THE SOLID PHASE EXTRACTION TECHNIQUE TO THE ANALYSIS OF BLOOD FOR THE PRESENCE OF NARCOTIC AND PHARMACEUTICAL SUBSTANCES

To cite this article:

Kataev SS, Dvorskaia ON. The application of the solid phase extraction technique to the analysis of blood for the presence of narcotic and pharmaceutical substances. Forensic Medical Expertise. 2012;55(4):38‑42. (In Russ.)

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This paper is devoted to the application of the solid phase extraction (SFE) technique based on the use of the SampliQ Evidex cartridges prepacked with a mixed phase "granular" sorbent for the screening of pharmaceuticals and narcotic substances in the whole blood by means of gas chromatography and mass-spectrometry. It is concluded based on the available data that the solid phase extraction technique has advantages over the traditional liquid-liquid extraction and may be used for the purpose of forensic chemical examination carried out in Bureaus of Forensic Medical Expertise.

Keywords:

solid phase extraction
screening of pharmaceuticals and narcotic substances
gas chromatography and mass-spectrometr

Authors:

Kataev S.S.

Permskoe kraevoe biuro sudebno-meditsinskoĭ ékspertizy

Dvorskaia O.N.

Permskaia gosudarstvennaia farmatsevticheskaia akademiia

List of references:

  1. Drummer O.H. Chromatographic screening techniques in systematic toxicological analysis. J Chromatography B 1999; 733: Issues 1-2: 27-45.
  2. Rittner M., Pragst F., Bork W.R., Neumann J. Screening method for seventy psychoactive drugs or drug metabolites in serum based on high-performance liquid chromatography - electrospray ionization mass spectrometry. J Anal Toxicol 2001; 25: 2: 115-124.
  3. Takeda A., Tanaka H., Shinohara T., Ohtake I. Systematic analysis of acid, neutral and basic drugs in horse plasma by combination of solid-phase extraction, non-aqueous partitioning and gas chromatography-mass spectrometry. J Chromatography B 2001; 758: Issues 2: 235-248.
  4. Dvorskaya O.N., Kataev S.S. Sravnenie effektivnosti zhidkost'-zhidkostnoi i tverdofaznoi ekstraktsii lekarstvennykh veshchestv na diskakh serii SPEC MR3. V kn.: Dostizheniya i perspektivy v oblasti sozdaniya novykh lekarstvennykh sredstv: Materialy. Perm' 2007; 172-177.
  5. Dvorskaya O.N., Kataev S.S., Sungatullina R.R. Effektivnost' ekstraktsii lekarstvennykh veshchestv na diskakh dlya TFE serii SPEC S18 i MR3. Vestn Permskoi gos farmatsevt akademii 2007; 2: 133-136.

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