Determination of morphine and codeine in forensic chemical studies with the use of a single quadrupole mass-selective detector coupled to the HPLC system

Barsegian S.S.; Purvina E.A.; Salomatin E.M.; Sviridova T.A.; Fedorova T.N.

doi:https://doi.org/

Barsegian S.S.

Biuro sudebno-meditsinskoĭ ékspertizy Departamenta zdravookhraneniia Moskvy

Purvina E.A.

Biuro sudebno-meditsinskoĭ ékspertizy Departamenta zdravookhraneniia Moskvy

Salomatin E.M.

FGBU "Rossiĭskiĭ tsentr sudebno-meditsinskoĭ ékspertizy" Minzdravsotsrazvitiia Rossii, Moskva

Sviridova T.A.

Biuro sudebno-meditsinskoĭ ékspertizy Departamenta zdravookhraneniia Moskvy

Fedorova T.N.

FGBU "Nauchnyĭ tsentr nevrologii RAMN", Moskva

Determination of morphine and codeine in forensic chemical studies with the use of a single quadrupole mass-selective detector coupled to the HPLC system

Authors:

Barsegian S.S., Purvina E.A., Salomatin E.M., Sviridova T.A., Fedorova T.N.

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Journal: Forensic Medical Expertise. 2012;55(6): 33‑37

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To cite this article:

Barsegian SS, Purvina EA, Salomatin EM, Sviridova TA, Fedorova TN. Determination of morphine and codeine in forensic chemical studies with the use of a single quadrupole mass-selective detector coupled to the HPLC system. Forensic Medical Expertise. 2012;55(6):33‑37. (In Russ.)

Подписка 2026 Судебно-медицинская экспертиза (Forensic Medical Expertise)

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Abstract:

It was shown that a single quadrupole mass-selective detector coupled to the HPLC system can be used in forensic chemical practice for the detection and quantitative measurement of morphine and codeine in forensic in various biological objects. An algorithm for the reliable identification of opiates in a concentration range starting from 0.002 mg% with a relative error below 20% (mean ca 9.5%) is proposed.

Keywords:

a single quadrupole mass-selective detector

HPLC

morphine

codeine

quantitative determination

forensic chemical studies.

Authors:

Barsegian S.S.

Biuro sudebno-meditsinskoĭ ékspertizy Departamenta zdravookhraneniia Moskvy

Purvina E.A.

Biuro sudebno-meditsinskoĭ ékspertizy Departamenta zdravookhraneniia Moskvy

Salomatin E.M.

FGBU "Rossiĭskiĭ tsentr sudebno-meditsinskoĭ ékspertizy" Minzdravsotsrazvitiia Rossii, Moskva

Sviridova T.A.

Biuro sudebno-meditsinskoĭ ékspertizy Departamenta zdravookhraneniia Moskvy

Fedorova T.N.

FGBU "Nauchnyĭ tsentr nevrologii RAMN", Moskva

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References:

http://www.interlab.ru/catalog/show.php?id=149
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